Analysis of twinned crystals
Collected on Rigaku's RAPID II, the
monoclinic crystals are twinned by a twin law that results in a 180°
rotation about the c axis. The two components of this particular sample
existed in an approx 80:20 ratio. The cadmium complex forms infinite
chains along the b-axis; the Cd centers are bridged by SO4 groups.

The twin components were indexed and integrated with the Rigaku TwinSolve package; the structure was refined using the twin-handling capabilities of SHELXL.
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Formula: |
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Formula weight: |
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Space group: |
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Unit cell: |
a = 18.28960 Å |
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Radiation: |
Mo-Kα |
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R1: |
0.0737 for 9770 Fo > 4σ(Fo) |
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Data collection temperature: |
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Source: |